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A Simple, Efficient, Catalyst-Free and Solvent-Less Microwave-Assisted Process for N-Cbz Protection of Several Amines

대한화학회지 2017년 61권 4호 p.151 ~ 156
 ( Aouf Zineb ) - Badji Mokhtar University Science Faculty Department of Chemistry

 ( Mansouri Rachida ) - Badji Mokhtar University Science Faculty Department of Chemistry
 ( Lakrout Salah ) - Badji Mokhtar University Science Faculty Department of Chemistry
 ( Berredjem Malika ) - Badji Mokhtar University Science Faculty Department of Chemistry
 ( Aouf Nour-Eddine ) - Badji Mokhtar University Science Faculty Department of Chemistry

Abstract


A simple, green and chemo-selective method for the N-benzyloxycarbonylation of amines, β-amino alcohols, α- amino esters and sulfonamides has been developed under microwave irradiation. Good to excellent yields of the N-benzyloxycarbamates compounds were obtained in short times without any side products.

키워드

Amine; Benzyl chloroformate (Cbz-Cl); Protection; Microwave-assisted; Solvent-free
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