medric medric
[닫기]
잠시만 기다려 주세요. 로딩중입니다.

One Pot Four-Component Synthesis of Novel Substituted 2-Phenyl-4(3H) Quinazolinones Using Recyclable Nanocrystalline CuMnO3 Catalyst

대한화학회지 2017년 61권 4호 p.157 ~ 162
 ( Borhade A. V. ) - HPT Arts and RYK Science College Department of Chemistry

 ( Tope D. R. ) - HPT Arts and RYK Science College Department of Chemistry
 ( Gare G. D. ) - HPT Arts and RYK Science College Department of Chemistry
 ( Dabhade G. B. ) - HPT Arts and RYK Science College Department of Chemistry

Abstract


In the present study, nanocrystalline mixed metal oxide, CuMnO3 catalyst have been synthesized by mechanochemical method with green chemistry approach. The synthesized catalyst was characterized by analytical techniques including FTIR, XRD, SEM, TEM and BET surface area. The synthesized catalyst shows high surface area is 121.06 m2/g with particle size 18 nm. The one pot four component synthesis of substituted 2-phenyl-4(3H) quinazolinone from the reaction of anthranilic acid, benzoyl chloride, hydrazine hydrate and substituted benzaldehyde in presence of CuMnO3 nanocatalyst has been carried out. It affords the corresponding products with high yield (76-95%) in very short reaction time. All the obtained products were characterized with 1HNMR, 13CNMR, FTIR and EIMS.

키워드

Green synthesis; Mixed metal oxide; Multicomponent reaction; 2-Phenyl-4(3H) quinazolinone; Recyclable catalyst
원문 및 링크아웃 정보
등재저널 정보
KCI